论文标题

钛中应力松弛的原位同步加速器衍射研究:温度和氧气对寒冷疲劳的影响

An in-situ synchrotron diffraction study of stress relaxation in titanium: Effect of temperature and oxygen on cold dwell fatigue

论文作者

Xiong, Yi, Karamched, Phani S., Nguyen, Chi-Toan, Collins, David M., Grilli, Nicolo, Magazzeni, Christopher M., Tarleton, Edmund, Wilkinson, Angus J.

论文摘要

有一个长期存在的技术问题,在室温下,在室温下循环载荷期间的压力居住会导致显着的疲劳寿命降低。据认为,在软晶粒中,局部依赖性的可塑性以易于定向的塑料滑动导致负载脱落,并且在附近的硬晶粒内的压力增加,以使其面向易于滑动。量化这段时间的依赖性可塑性过程是了解复杂的冷藏疲劳问题的关键。了解工作温度和氧气含量对寒冷疲劳的影响将对未来的合金设计有益于解决此问题。在这项工作中,使用在应力松弛实验期间的X射线衍射来表征两个在4种不同温度下(室温,75C,145C和250C)在4种不同温度下具有不同氧气含量的商业纯钛样品(1级和4级)的塑性行为。通过跟踪从多个晶体平面家族(21衍射环)跟踪其方向相对于载荷方向的函数来测量晶格菌株。通过将晶体可塑性有限元模型拟合到沿载荷轴沿载荷轴的晶格菌株释放响应拟合,以五个强反射测量的晶格可塑性有限元模型,以对棱镜和基础滑移建立了临界分辨剪应力,激活能量和激活体积。发现较高的应变速率灵敏度会导致寒冷期间较高的可塑性。

There is a long-standing technological problem in which a stress dwell during cyclic loading at room temperature in Ti causes a significant fatigue life reduction. It is thought that localised time dependent plasticity in soft grains favourably oriented for easy plastic slip leads to load shedding and an increase in stress within a neighbouring hard grain poorly oriented for easy slip. Quantifying this time dependent plasticity process is key to understand the complex cold dwell fatigue problem. Knowing the effect of operating temperature and oxygen content on cold dwell fatigue will be beneficial for future alloy design to address this problem. In this work, synchrotron X-ray diffraction during stress relaxation experiments was used to characterise the time dependent plastic behaviour of two commercially pure titanium samples (grade 1 and grade 4) with different oxygen content at 4 different temperatures (room temperature, 75C, 145C and 250C). Lattice strains were measured by tracking the diffraction peak shift from multiple crystallographic plane families (21 diffraction rings) as a function of their orientation with respect to the loading direction. Critical resolved shear stress, activation energy and activation volume were established for both prismatic and basal slip as a function of temperature and oxygen content by fitting a crystal plasticity finite element model to the lattice strain relaxation responses measured along the loading axis for five strong reflections. Higher strain rate sensitivity was found to lead to higher plasticity during cold dwell.

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